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http://www.dsse.biz/equipment/sweetener/hydrogenator
The DSSE Hydrogenator works under a pressure of approximately 50 bar (g) and a temperature of 140ºC. The process is batch-wise and the total time per charge amounts to 5-8 hours depending on the process design. The reaction takes place theoretically as follows: C 6 H 12 O 6 + H 2-> C 6 H 14 O 6 + 57.4 kJoule/kmol
https://www.ekato.com/solutions/processes/hydrogenation/
A manufacturer of specialty chemicals for the paint industry was able to determine through tests in the hydrogenation pilot plant at EKATO in Schopfheim, Germany, that it is possible to reduce the catalyst loading from 2.5% to 1.0% and the reaction time from four to two hours if the dispersion of the hydrogen and the cooling capacity of the reactor are improved.
https://hydrogenator.business.site/
Hydrogenator, Grease Kettle, Hydrogen Plant Manufacturer, India Opening at 9:30 AM tomorrow WhatsApp 075067 70210 Call 075067 70210 Get directions Message 075067 70210 Contact Us Get Quote Find Table Make Appointment Place Order View Menu
http://ccc.chem.pitt.edu/wipf/Web/H-Cube%20presentation.pdf
Scale 3-5 g, 1-2 hours 60-70% Yield, 95% NMR Batch reaction took 3 days with incomplete conversion! Difficult to reduce stable aromatic heterocycles. Hydrogenation without dehalogenation Mild conditions to avoid dechlorination! T [¡C ] …
https://www.erowid.org/archive/rhodium/chemistry/mdma.catalytic.html
When addition was complete 400g of anhydrous silica gel was added and overhead stirring was commenced for 6 hours. The silica gel was filtered off and 100g of 10% Pt/C was added to the mix. This was then placed in a hydrogenator and shaken for 4 hours, at which point 105% of the theoretical H2 had been absorbed.
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